The IPD3000, Imaging Plate Diffractometer, is designed for a complete diffractometric analysis without the need of any motor nor any electronic detector. The measurement is obtained by means of imaging plates (they can be used thousands of times!), on which the diffracted rays are revealed thanks to phosphors. A single complete diffractogram can be realised in few minutes!

Imaging Plates are nearly ideal photon detectors that give you highest quality digital images. They replace the old films and can be reused thousands of time.

The collected images can be read by the program MAUD. An high dynamic range and a great sensitivity of the imaging plates ensure resolution and quality of the spectra!  

The Imaging Plate is a flexible image sensor in which bunches of very small crystals (grain size: about 5 µm) of photo-stimulable phosphor of barium fluorobromide containing a trace amount of bivalent europium as a luminescence center, formulated as BaFBr: Eu2+, are uniformly coated on a polyester support film. 

Exposure of samples to the Imaging Plate is performed in a manner similar to that of photo-film. The exposed Imaging Plate is scanned with a laser beam of red light while the plate is being conveyed with high accuracy in a phosphor reader. 

The exposed Imaging Plate, while being conveyed, is scanned with a focused laser beam. The PSL released upon the laser is collected into the photomultiplier tube (PMT) through the light collection guide and is converted to electric signals.
 

Examples of applications

1) Cement industry

the image collected with IPD3000

the corresponding diffractogram analysed with MAUD.


2a) Roman coins

A Silver roman coin: image obtained with the IPD 3000

The corresponding diffractogram, analysed with MAUD

2b) Roman coins

A Silver coin with a corrosive product

The corresponding diffractogram, analysed with MAUD


3) Texture analysis on polypropylene wires

Found strong fiber texture (pole figures plotted in log scale) along (001) corresponding to the direction of the polymer chains as expected.

The fiber dispersion in this case was refined with MAUD program using a standard texture function; the mean angular deviation from the fiber axis was: 16.5 (± 0.05) deg. This method can be used to measure accurately the texture of epitaxial films and their perfection etc.

Mean domain size of 82 Angstrom and 0.019 the r.m.s. microstrain corresponding to paracrystallinity disorder. 

Crystal structure and cell parameters were refined as well.

The image collected with IPD 3000

One of the corresponding diffractograms

Polar figures relative to three planes

The crystallite size (and paracrystallinity) as analyzed with MAUD.

 

Click Here to see the IPD 3000 Standard configuration

 
 

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